HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzamide → 1-(5-bromo-2,3-dimethoxyphenyl)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzamide | HCID 2331 | — |
| Reactant | 5-bromo-2,3-dimethoxybenzoic acid | HCID 322872 | — |
| Product | 1-(5-bromo-2,3-dimethoxyphenyl)ethanone | HCID 344484 | — |
Reaction Steps
5-Bromo-2,3-dimethoxybenzoic acid (2 g) was converted to the benzamide derivative analogously to O3.043, and the latter to the title compound analogously to O2.059. 1.1 g of the title compound were obtained. LC-MS rt: 3.70 min [M+H]+: 259.0 (met. d)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08198272B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-6e1058fce57b48fab23dee0c4197cbb2 |
| Source note | uspto-grants-2012_06 |