Benzamide → HCID 21192648, compound

HRID 217730Notes

Reaction equation

[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([O:13][CH3:14])[C:10]=1[O:11][CH3:12])[C:5]([OH:7])=O.[C:15](N)(=O)C1C=CC=CC=1>>[Cl:1][C:2]1[CH:3]=[C:4]([C:5](=[O:7])[CH3:15])[CH:8]=[C:9]([O:13][CH3:14])[C:10]=1[O:11][CH3:12]

Participants

Reactant 2

HCID 2331Benzamide

HCID 2400533-Chloro-4,5-dimethoxybenzoic acid

Product 1

HCID 21192648HCID 21192648, compound

Procedure

3-Chloro-4,5-dimethoxybenzoic acid (1 g) was converted to the benzamide derivative analogously to O3.043, and the latter to the title compound analogously to O2.059. 495 mg of the title compound were obtained. LC-MS rt: 1.55 min [M+H]+: 215.1 (met. a)

Sources & evidence

ORD record: ord-7441587f7f4c4211a83df5f54d8fdd34
Source dataset: uspto-grants-2012_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08198272B2

Reaction notes

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