Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | L-Malic Acid | HCID 222656 | — |
| Reactant | Sunitinib | HCID 5329102 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Sunitinib Malate | HCID 6456015 | — |
Reaction Steps
To Sunitinib base (300 mg), L-malic acid (101 mg), and AcOEt (10 ml) are added, the mixture is heated to 77° C. for 10 min, after precipitation the obtained solid is filtered, dried on air.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09067915B2 |
|---|
| Source dataset | uspto-grants-2015_06 |
|---|
| ORD ID | ord-0a747c2b7a96487f8f6e195e02168bbb |
|---|
| Source note | uspto-grants-2015_06 |
|---|
