Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sunitinib | HCID 5329102 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86653606 | HCID 86653606 | — |
Reaction Steps
A solution of Sunitinib acetate was prepared in the following way: 10 g Sunitinib Base (1 eq) was suspended in 50 ml of water, then 1.58 g (1.05 eq) of acetic acid was added under stirring obtaining a solution. This solution was heated to 60° C. Then 160 ml of ethanol were added at this temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09067915B2 |
|---|
| Source dataset | uspto-grants-2015_06 |
|---|
| ORD ID | ord-b01c5ffe0148466f8dd36a8be647d638 |
|---|
| Source note | uspto-grants-2015_06 |
|---|
