2,3-Dichlorobenzoic acid → HCID 90409660, compound

HRID 2177611Notes

Reaction equation

HRID 2177611 reaction equation
[CH3:1][CH:2]1[NH:7][CH2:6][C:5]2[N:8]=[N:9][N:10]([C:11]3[CH:16]=[CH:15][CH:14]=[CH:13][N:12]=3)[C:4]=2[CH2:3]1.[Cl:17][C:18]1[C:26]([Cl:27])=[CH:25][CH:24]=[CH:23][C:19]=1[C:20](O)=[O:21]>>[Cl:17][C:18]1[C:26]([Cl:27])=[CH:25][CH:24]=[CH:23][C:19]=1[C:20]([N:7]1[CH:2]([CH3:1])[CH2:3][C:4]2[N:10]([C:11]3[CH:16]=[CH:15][CH:14]=[CH:13][N:12]=3)[N:9]=[N:8][C:5]=2[CH2:6]1)=[O:21]

Participants

3

Reactant 2

HCID 57652,3-Dichlorobenzoic acidHCID 90408482HCID 90408482, compound

Product 1

HCID 90409660HCID 90409660, compound

Procedure

Example 120 was prepared from 6-methyl-1-(pyridin-2-yl)-4,5,6,7-tetrahydro-1H-[1,2,3]triazolo[4,5-c]pyridine and 2,3 dichlorobenzoic acid using the conditions described in Example 65. MS (ESI) mass calcd. C18H15Cl2N5O, 387.07. m/z found, 388.1 [M+H]+.

Sources & evidence

ORD record
ord-356c8c1245054bc6a4ed90a6bd898dd9
Source dataset
uspto-grants-2015_06
Patent number
US09066946B2

Reaction notes

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