HCID 67107511, compound → HCID 52914081, compound

HRID 2177669Notes

Reaction equation

HRID 2177669 reaction equation
[C:1]1([S:7]([CH2:10][C:11]2[C:16]([C:17]([O:19]C)=[O:18])=[C:15]([O:21][CH3:22])[C:14]([C:23]3[CH:24]=[N:25][S:26][CH:27]=3)=[CH:13][CH:12]=2)(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>CO>[C:1]1([S:7]([CH2:10][C:11]2[C:16]([C:17]([OH:19])=[O:18])=[C:15]([O:21][CH3:22])[C:14]([C:23]3[CH:24]=[N:25][S:26][CH:27]=3)=[CH:13][CH:12]=2)(=[O:9])=[O:8])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

3

Reactant 1

HCID 67107511HCID 67107511, compound2×

Product 1

HCID 52914081HCID 52914081, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Prepared by proceeding in a similar manner to Example 3, starting from crude methyl 6-(benzenesulphonylmethyl)-3-(isothiazol-4-yl)-2-methoxybenzoate (Intermediate 57) using methanol in place of dioxane.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-13f215681a654aaca2c7c948fb1ccf12
Source dataset
uspto-grants-2015_06
Patent number
US09067905B2

Reaction notes

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