HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl N-(2-bromoethyl)carbamate → Methyl 2-[2-(t-butoxycarbonyl)aminoethoxy]-6-(4-fluorobenzenesulphonyl-methyl)-3-(furan-3-yl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl N-(2-bromoethyl)carbamate | HCID 4103526 | — |
| Reactant | Ethyl 6-(benzenesulphonylmethyl)-2-[2-(t-butoxycarbonyl)aminoethoxy]-3-(furan-3-yl)benzoate | HCID 67107565 | — |
| Reactant | Methyl 6-(4-fluorobenzenesulphonylmethyl)-3-(furan-3-yl)-2-hydroxybenzoate | HCID 67108009 | — |
| Product | Methyl 2-[2-(t-butoxycarbonyl)aminoethoxy]-6-(4-fluorobenzenesulphonyl-methyl)-3-(furan-3-yl)benzoate | HCID 67107508 | — |
Reaction Steps
Prepared by proceeding in a similar manner to Intermediate 10, starting from methyl 6-(4-fluorobenzenesulphonylmethyl)-3-(furan-3-yl)-2-hydroxybenzoate (Intermediate 38) and 2-[N-(t-butoxycarbonyl)amino]ethyl bromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067905B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-3ffc55065d5c420fa09b67aac82c3a98 |
| Source note | uspto-grants-2015_06 |