HRID2177771

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID4103526

tert-Butyl N-(2-bromoethyl)carbamate

C7H14BrNO2

结构：CCOC(=O)c1c(CS(=O)(=O)c2ccccc2)ccc(-c2ccoc2)c1OCCNC(=O)OC(C)(C)C

HCID67107565

未命名化合物

结构：CCc1ccc(CS(=O)(=O)c2ccccc2)c(C(=O)OC)c1O

HCID67107635

未命名化合物

2 次

PRODUCTS

生成物

结构：CCc1ccc(CS(=O)(=O)c2ccccc2)c(C(=O)OC)c1OCCNC(=O)OC(C)(C)C

HCID67107759

未命名化合物

PROCEDURE

实验过程

Prepared by proceeding in a similar manner to Intermediate 10, starting from methyl 6-(benzenesulphonylmethyl)-3-ethyl-2-hydroxybenzoate (Intermediate 110) and 2-(t-butoxycarbonylamino)ethyl bromide

WORKUP

后处理

customPrepared

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-6ee9702fe16848c982704ef00fc12938
来源数据集: uspto-grants-2015_06
DOI: 10.6084/m9.figshare.5104873.v1
专利: US09067905B2
来源说明: uspto-grants-2015_06

反应 SMILES

[C:1]1([S:7]([CH2:10][C:11]2[C:16]([C:17]([O:19][CH2:20]C)=[O:18])=[C:15]([O:22][CH2:23][CH2:24][NH:25][C:26]([O:28][C:29]([CH3:32])([CH3:31])[CH3:30])=[O:27])[C:14]([C:33]3C=CO[CH:34]=3)=[CH:13][CH:12]=2)(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C1(S(CC2C(C(OC)=O)=C(O)C(CC)=CC=2)(=O)=O)C=CC=CC=1.C(OC(NCCBr)=O)(C)(C)C>>[C:1]1([S:7]([CH2:10][C:11]2[C:16]([C:17]([O:19][CH3:20])=[O:18])=[C:15]([O:22][CH2:23][CH2:24][NH:25][C:26]([O:28][C:29]([CH3:31])([CH3:30])[CH3:32])=[O:27])[C:14]([CH2:33][CH3:34])=[CH:13][CH:12]=2)(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1