HCID 67107433, compound → HCID 67107686, compound

HRID 2177834Notes

Reaction equation

HRID 2177834 reaction equation
C(N(CC)CCCC1C=CC=CC=1S(CC1C(C(OC)=O)=C(OC)C(C2C=COC=2)=CC=1)(=O)=O)C.[C:36]1([S:42]([CH2:45][C:46]2[CH:55]=[CH:54][C:53]3[C:48](=[C:49]([O:57][CH3:58])[CH:50]=[CH:51][C:52]=3Br)[C:47]=2[C:59]([O:61][CH3:62])=[O:60])(=[O:44])=[O:43])[CH:41]=[CH:40][CH:39]=[CH:38][CH:37]=1>>[C:36]1([S:42]([CH2:45][C:46]2[CH:55]=[CH:54][C:53]3[C:48](=[C:49]([O:57][CH3:58])[CH:50]=[CH:51][CH:52]=3)[C:47]=2[C:59]([O:61][CH3:62])=[O:60])(=[O:44])=[O:43])[CH:37]=[CH:38][CH:39]=[CH:40][CH:41]=1

Participants

3

Reactant 2

HCID 67107433HCID 67107433, compoundHCID 67107562HCID 67107562, compound2×

Product 1

HCID 67107686HCID 67107686, compound

Procedure

Prepared by proceeding in a similar manner to Intermediate 4, starting from methyl 2-(benzenesulphonylmethyl)-5-bromo-8-methoxynaphthalene-1-carboxylate (Intermediate 188), as a white solid.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-6c46c8f709574e8f83a75341406f3d6c
Source dataset
uspto-grants-2015_06
Patent number
US09067905B2

Reaction notes

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