HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-1,2-dichlorobenzene → 1-(3,4-Dichlorophenyl)-2-phenylethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-1,2-dichlorobenzene | HCID 29013 | — |
| Reactant | 1-(3,5-Dichlorophenyl)-2-phenylethanone | HCID 2758146 | — |
| Product | 1-(3,4-Dichlorophenyl)-2-phenylethanone | HCID 2758145 | 42.4% |
Reaction Steps
Prepared following the procedure described in Intermediate 13, starting from 4-bromo-1,2-dichlorobenzene, where the crude product was purified by column chromatography (PE:EtOAc=100:1) to afford Intermediate 19 (230 mg, yield 42.4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067893B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-0a8d61b6413c4f1e8b2cd4b88b2d2a5b |
| Source note | uspto-grants-2015_06 |