HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Cyano-4-fluorobenzenesulfonyl chloride → HCID 117653235, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Cyano-4-fluorobenzenesulfonyl chloride | HCID 2778908 | — |
| Reactant | HCID 47283228 | HCID 47283228 | — |
| Product | HCID 117653235 | HCID 117653235 | — |
Reaction Steps
The title compound was prepared according to the method described for Preparation 18 using 6-((2,4-dimethoxybenzyl)amino)nicotinonitrile (Preparation 37) and 3-cyano-4-fluorobenzene-1-sulfonyl chloride. The residue was purified by reverse phase chromatography eluting with 0-100% MeCN in water/0.1% formic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067922B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-5dce1a58abc342b39239e668a783e922 |
| Source note | uspto-grants-2015_06 |