HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 67953996, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 67966902 | HCID 67966902 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67953996 | HCID 67953996 | — |
Reaction Steps
Compound 15-B (0.500 g, 1.77 mmol) was dissolved in 4N HCl in dioxane (17.75 mL) and methanol (12 mL) and the reaction mixture was stirred for 3 h at room temperature. The solvent was evaporated in vacuo to give compound 16-A as a light yellow solid; MS m/z (M+H+) 182.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067935B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-fffb57ccc0e049e28e5478404d94488d |
| Source note | uspto-grants-2015_06 |