HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59212643, compound → HCID 59212620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59212643 | HCID 59212643 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 59212620 | HCID 59212620 | — |
Reaction Steps
The intermediate obtained from step E (0.23 g) was dissolved in a solution of 4 N HCl in dioxane (3 mL). After being stirred at room temperature for 2 h, the solution was concentrated to provide the title compound as a trihydrochloride salt (0.23 g). MS calculated for C20H30BrN3: (M+H)+392; found 392.2, 394.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09067921B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-30315f8ff283462b97be53cd57fc24c0 |
| Source note | uspto-grants-2015_06 |