HRID217966
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
2.4 g of 2-(1-(2-methoxyethyl)piperidin-4-ylidene)acetic acid was dissolved in 20 mL of thionyl chloride, refluxed for 2 hours, evaporated in vacuo to remove thionyl chloride and give a solid product.
WORKUP
后处理
- temperaturerefluxed for 2 hours
- customevaporated in vacuo
- customto remove thionyl chloride
- customgive a solid product