HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-(4-Methoxy-3-nitrophenyl)propan-2-one → 3-Amino-4-methoxyphenylacetone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-(4-Methoxy-3-nitrophenyl)propan-2-one | HCID 22488977 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 3-Amino-4-methoxyphenylacetone | HCID 20747900 | 94% |
Reaktionsschritte
The mixture of compound 10 (3.0 g, 14.3 mmol) and 10% palladium on carbon (1.6 g) in ethanol (230 ml) was stirred under hydrogen for 3 hours. Filtration of the catalyst and evaporation of solvent gave desired product 11 (2.41 g, 94%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06887867B2 |
| Quelldatensatz | uspto-grants-2005_05 |
| ORD ID | ord-d3e420440800475dbf88c7b2e28ae43e |
| Quellennotiz | uspto-grants-2005_05 |