2,5-Dibromopyridine → HCID 86759698, compound
Reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5](Br)=[CH:4][N:3]=1.COCN[C:13](=[O:24])[CH2:14][CH2:15][NH:16][C:17](=[O:23])[O:18][C:19]([CH3:22])([CH3:21])[CH3:20]>>[Br:1][C:2]1[N:3]=[CH:4][C:5]([C:13](=[O:24])[CH2:14][CH2:15][NH:16][C:17](=[O:23])[O:18][C:19]([CH3:20])([CH3:21])[CH3:22])=[CH:6][CH:7]=1Participants
3
Procedure
The sub-title compound was prepared from 2,5-dibromopyridine and [3-(methoxymethylamino)-3-oxopropyl carbamic acid, 1,1-dimethylethyl ester by the method of Example 58(a).
Sources & evidence
- ORD record
- ord-cfe96f058d2a4ab09cf27400c1ecb73f
- Source dataset
- uspto-grants-2005_05
- Patent number
- US06887871B2
Reaction notes
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