Phenol, 5-chloro-2-nitro- → HCID 86759702, compound

HRID 2179977Notes

Reaction equation

HRID 2179977 reaction equation
[CH3:1][C:2]([O:5][C:6](=[O:19])[N:7]([CH2:9][CH2:10][C@H:11]([OH:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[CH3:8])([CH3:4])[CH3:3].[Cl:20][C:21]1[CH:22]=[CH:23][C:24]([N+:28]([O-:30])=[O:29])=[C:25](O)[CH:26]=1>>[Cl:20][C:21]1[CH:26]=[CH:25][C:24]([N+:28]([O-:30])=[O:29])=[C:23]([CH:22]=1)[O:18][C@@H:11]([C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1)[CH2:10][CH2:9][N:7]([CH3:8])[C:6](=[O:19])[O:5][C:2]([CH3:1])([CH3:3])[CH3:4]

Participants

3

Reactant 2

HCID 11900Phenol, 5-chloro-2-nitro-HCID 11043680HCID 11043680, compound

Product 1

HCID 86759702HCID 86759702, compound

Procedure

This was prepared by the method of Example 20(a) using [(3S)-3-hydroxy-3-phenylpropyl]methylcarbamic acid 1,1-dimethylethyl ester and 5-chloro-2-nitrophenol.

Workup

  1. customThis was prepared by the method of Example 20(a)

Sources & evidence

ORD record
ord-cae1c6948e764158a17682312c803008
Source dataset
uspto-grants-2005_05
Patent number
US06887871B2

Reaction notes

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