Hydrazine → HCID 21554741, compound

HRID 21803Notes

Reaction equation

HRID 21803 reaction equation
[NH2:1]N.[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11]C1C=CC=C2C(NC(=O)C=12)=O>CO>[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][NH2:1]

Participants

4

Reactant 2

HCID 9321HydrazineHCID 544460722-(N-methylpiperazinyl)ethylphthalimide

Product 1

HCID 21554741HCID 21554741, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 2-(N-methylpiperazinyl)ethylphthalimide (218 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

Workup

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

Sources & evidence

ORD record
ord-81144ce9d9054fa5ae7fdc113d564caa
Source dataset
uspto-grants-1995_06
Patent number
US05424451

Reaction notes

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