Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzenecarbodithioic acid → Bis(thiobenzoyl) Disulfide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzenecarbodithioic acid | HCID 67141 | — |
| 반응물 | Potassium triiodide | HCID 105053 | — |
| 반응물 | Sodium | HCID 5360545 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | Bis(thiobenzoyl) Disulfide | HCID 10902862 | — |
반응 단계
100 ml of a sodium salt solution of dithiobenzoic acid (0.15 mol) were added by drops to an 80 not iodine aqueous solution (0.1 mol) over 1 hour. After completing the reaction, the obtained product was dissolved in an organic solvent of tetrahydrofurane (THF) and washed with distillated water twice and dried over magnesium sulfate (MgSO4). The organic solvent was removed by vacuum evaporation. It was then recrystalized in ethanol to obtain dithiobenzoyl disulfide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06888020B2 |
| 출처 데이터셋 | uspto-grants-2005_05 |
| ORD ID | ord-c850d229e6554770a472de0d406a2346 |
| 출처 메모 | uspto-grants-2005_05 |