Sodium Hydroxide → HCID 22491066, compound

Participants

Reaction Steps

Following General Procedure G, ethyl 7-(7-ethoxy-2,2,4-trimethyl-2H-chromen-6-yl)-3-methyl-nona-2E,4E,6Z-trienoate (Compound 36, 33 mg, 0.086 mmol) was hydrolyzed with 1M NaOH. Purification by column chromatography (silica gel, 30% ethyl acetate in hexanes) followed by recrystallization from acetonitrile gave rise to the title compound as a light yellow solid.

Provenance & Evidence