HRID2180521

反应详情

EQUATION

反应方程式

REACTANTS

反应物

$反应SMILES：CCOC(=O)/C=C(\C)CP(=O)(OCC)OCC$

HCID6000084

未命名化合物

反应SMILES：CCCCOc1cc2c(cc1/C(C)=C(/F)C=O)C(C(C)C)=CC(C)(C)O2

HCID22490854

未命名化合物

2 次

PRODUCTS

产物

$反应SMILES：CCCCOc1cc2c(cc1\C(C)=C(F)/C=C/C(C)=C/C(=O)OCC)C(C(C)C)=CC(C)(C)O2$

HCID86759710

未命名化合物

PROCEDURE

实验过程

Following General Procedure O, ethyl 4-(diethoxyphosphoryl)-3-methyl-but-2E-enoate (183 mg, 0.70 mmol) and (2E)-3-(7-butoxy-4-isopropyl-2,2-dimethyl-2H-chromen-6-yl)-2-fluoro-but-2-enal (Compound 100, 86 mg, 0.24 mmol) were reacted to give the title compound as a yellow oil after purification by flash chromatography (silica gel, 5% ethyl acetate in hexane).

WORKUP

后处理

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