HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 60003033, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 87972539 | HCID 87972539 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 60003033 | HCID 60003033 | — |
Reaction Steps
Following General Procedure G, a solution of ethyl 6-fluoro-7-(7-methoxy-2,2,4-trimethyl-2H-chromen-6-yl)-3-methyl-nona-2E,4E,6E-trienoate (Compound 116,204 mg, 0.51 mmol) in ethanol and THF was hydrolyzed with 1M NaOH. Purification by flash chromatography (silica gel, 75:25 hexane/ethyl acetate) afforded the title compound as a light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06887896B1 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-8f867a34b01440a593b0140f755112bd |
| Source note | uspto-grants-2005_05 |