HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl 2-fluoro-2-phosphonoacetate → HCID 86597836, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl 2-fluoro-2-phosphonoacetate | HCID 2734865 | — |
| Reactant | HCID 22490812 | HCID 22490812 | — |
| Product | HCID 86597836 | HCID 86597836 | — |
Reaction Steps
Following General Procedure K, triethyl-2-fluoro-2-phosphonoacetate (0.4 mL, 2.14 mmol) and 1-(8-chloro-4-isopropyl-7-methoxy-2,2-dimethyl-2H-chromen-6-yl)-propan-1-one (Compound 140, 229 mg, 0.71 mmol) were reacted to give the title compound as a yellow oil after purification by flash chromatography (silica gel, 1:9 ethyl acetate/hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06887896B1 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-6b5594bec4104f5f849f986574bbfc23 |
| Source note | uspto-grants-2005_05 |