HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 22490945, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Methyl morpholine oxide | HCID 82029 | — |
| Reactant | HCID 22491054 | HCID 22491054 | — |
| Catalyst | HCID 178419074 | HCID 178419074 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 22490945 | HCID 22490945 | — |
Reaction Steps
As described in General Procedure H-1, (2E)-2-fluoro-3-(4,4-dimethyl-6-n-propoxy-1-isopropyl-3,4-dihydronaphthalen-7-yl)-2-butenol (Compound A-53, 0.024 g, 0.069 mmol), tetrapropylammonium perruthenate (0.012 g, 0.038 mmol) and 4-methylmorpholine N-oxide (0.022 g, 0.19 mmol) were reacted in acetonitrile (0.2 mL) and dichloromethane (1 mL) to produce the title compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06887896B1 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-267e571b2f7040faa0d6dd9d1157466f |
| Source note | uspto-grants-2005_05 |