Acetonitrile → HCID 22491023, compound

Participants

Reaction Steps

As described in General Procedure H-1, (2E)-2-fluoro-3-(4,4-dimethyl-6-(cyclopropyl)methoxy-1-isopropyl-3,4-dihydronaphthalen-7-yl)-2-butenol (Compound A-54, 0.025 g, 0.070 mmol), tetrapropylammonium perruthenate (0.012 g, 0.038 mmol) and 4-methylmorpholine N-oxide (0.022 g, 0.19 mmol) were reacted in acetonitrile (0.2 mL) and dichloromethane (1 mL) to produce the title compound as an oil.

Provenance & Evidence