Hydrazine → HCID 54275604, compound

HRID 21807Notes

Reaction equation

HRID 21807 reaction equation
[NH2:1]N.[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12][CH2:13]C1C=CC=C2C(NC(=O)C=12)=O>CO>[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12][CH2:13][NH2:1]

Participants

4

Reactant 2

HCID 9321HydrazineHCID 538263884-(N-methylpiperazinyl)butylphthalimide

Product 1

HCID 54275604HCID 54275604, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 4-(N-methylpiperazinyl)butylphthalimide (240 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

Workup

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

Sources & evidence

ORD record
ord-c944c58f544d4256941c6aa331ac25a9
Source dataset
uspto-grants-1995_06
Patent number
US05424451

Reaction notes

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