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HRID2180776

反应详情

EQUATION

反应方程式

HRID 2180776 反应方程式

REACTANTS

反应物

2
N-[(3,5-difluorophenyl)acetyl]alanine 分子结构式
HCID12135350

N-[(3,5-difluorophenyl)acetyl]alanine

C11H11F2NO3

HCID 22492067 分子结构式
HCID22492067

未命名化合物

PRODUCTS

产物

1
HCID 22894873 分子结构式
HCID22894873

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
HCID 21226129 分子结构式
溶剂HCID21226129

未命名化合物

PROCEDURE

实验过程

Following General Procedure A and using N-(3,5-difluorophenylacetyl)-L-alanine (from Example B2 above) and methyl 2-amino-3-methoxypropionate hydrochloride (Bachem), the title compound was prepared as a solid (mp=165-168° C.). The reaction was monitored by tlc (Rf=0.48 in 10% MeOH/DCM) and the product was purified by acid/base washes.

WORKUP

后处理

  1. customthe product was purified by acid/base washes