HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 5025990, compound → HCID 22894866, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 5025990 | HCID 5025990 | — |
| Reactant | (2S)-2-[[2-(3,5-difluorophenyl)acetyl]amino]propanoic acid | HCID 12135350 | — |
| Product | HCID 22894866 | HCID 22894866 | — |
Reaction Steps
Following General Procedure C and using N-(3,5-difluorophenylacetyl)-L-alanine (from Example B2 above) and ethyl 2-amino-2-(benzothiophen-2-yl)acetate [CAS No. 98800-64-7], the title compound was prepared as a solid (mp=189-190° C.). The product was purified by preparative LC 2000 chromatography using 2:8 EtOAc/hexanes as the eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06888022B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-dbe4adf7876d4ac4a66697640ed0c4f4 |
| Source note | uspto-grants-2005_05 |