HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Butane sultone → HCID 178506954, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Butane sultone | HCID 15411 | — |
| Reactant | tert-Butyl methyl ether | HCID 15413 | — |
| Reactant | Lithium hydroxide, monohydrate | HCID 168937 | — |
| Reactant | Perfluorobutanesulfonamide | HCID 10958205 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 178506954 | HCID 178506954 | 7% |
Reaction Steps
C4F9SO2N(H)C4H8SO3Li was prepared essentially according to the procedure described in Preparation 3 replacing C4F9SO2NH(C2H4OH) with C4F9SO2NH2 (15.0 g; 0.05 moles), and the corresponding amounts of the following were used: LiOH—H2O (2.32 g; 0.055 moles), MTBE (100 mL), DME (100 mL), and 1,4-butanesultone (7.5 g; 0.055 moles). A waxy white solid was isolated (1.57 g; 7% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06890452B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-92efabfe14294b5291a1c7cc7273902f |
| Source note | uspto-grants-2005_05 |