HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Ethoxy-3,5-dimethoxyphenyl)boronic acid → 1-Iodo-3,5-dimethoxy-4-(2-methoxyethoxy)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Ethoxy-3,5-dimethoxyphenyl)boronic acid | HCID 22485535 | — |
| Reactant | 4-Ethoxy-1-iodo-3,5-dimethoxybenzene | HCID 22485559 | — |
| Product | 1-Iodo-3,5-dimethoxy-4-(2-methoxyethoxy)benzene | HCID 22485561 | — |
| Product | 4-(2-Methoxyethoxy)-3,5-dimethoxyphenylboronic acid | HCID 22485615 | — |
Reaction Steps
Applying the synthetic procedure of 4-ethoxy-3,5-dimethoxyphenylboronic acid from 4-ethoxy-1-iodo-3,5-dimethoxybenzene in Reference Example 3, the title compound was obtained as a colorless amorphous powder (276.0 mg, yield: 54%) from 1-iodo-3,5-dimethoxy-4-(2-methoxyethoxy)benzene (673.0 mg, 2.00 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06890940B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-80da6ada744249bca2e34e0ce48ea4b2 |
| Source note | uspto-grants-2005_05 |