Hydrazine → 8-Pyrrolidinyloctylamine

HRID 21813Notes

Reaction equation

HRID 21813 reaction equation
[NH2:1]N.[N:3]1([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:7][CH2:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][NH2:1])[CH2:4][CH2:5][CH2:6][CH2:7]1

Participants

4

Reactant 2

HCID 9321HydrazineHCID 542934218-Pyrrolidinyloctylphthalimide

Product 1

HCID 199335008-Pyrrolidinyloctylamine

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 8-pyrrolidinyloctylphthalimide (263 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

Workup

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

Sources & evidence

ORD record
ord-57327deb27424964be85d1a8d0e252d6
Source dataset
uspto-grants-1995_06
Patent number
US05424451

Reaction notes

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