Methanol → HCID 22485625, compound

Participants

Reaction Steps

To a solution of N,N′-bis[2-(2,3-dimethoxyphenyl)-5-pyridyl]-N,N′-dimethylethylenediamine (33.0 mg, 0.0641 mmol) in chloroform (3.0 mL) was added a 1.0 M solution of methanesulfonic acid in methanol (0.13 mL, 0.13 mmol), and the reaction mixture was concentrated under reduced pressure. Methanol-diethyl ether was added to the residue and the resulting precipitate was collected by filtration to yield the title compound as a yellow crystalline powder (melting point: 191.5-194.5° C.)(39.5 mg, yield: 87%).

Provenance & Evidence