Methanesulfonic Acid → HCID 22485576, compound

Participants

Reaction Steps

To a solution of N,N′-bis[2-(2,6-dimethoxyphenyl)-5-pyridyl]-N,N′-dimethylethylenediamine (72.3 mg, 0.141 mmol) in methanol-chloroform (9:1, 10 mL) was added a 1.0 M aqueous methanesulfonic acid solution (0.35 mL, 0.35 mmol), and the reaction mixture was concentrated under reduced pressure. Ethanol (5.0 mL) was added to the residue, and the mixture was concentrated under reduced pressure. The residue was recrystallized from ethanol-diethyl ether to provide the title compound as a pale yellow crystalline powder (melting point: 243.0-245.0° C. )(94.1 mg, yield: 95%).

Provenance & Evidence