Methanol → HCID 22485603, compound

Participants

Reaction Steps

To a solution of N,N′-bis[2-(4-acetyl-3,5-dimethoxyphenyl)-5-pyridyl]-N,N′-dimethylethylenediamine (76.4 mg, 0.128 mmol) in chloroform (5.0 mL) was added a 1.0 M solution of methanesulfonic acid in methanol (0.32 mL, 0.32 mmol), and the reaction mixture was concentrated under reduced pressure. Chloroform-diethyl ether was added to the residue and the resulting precipitate was collected by filtration to yield the title compound as a yellow crystalline powder (melting point: 261.0-265.5° C.)(75.1 mg, yield: 74%).

Provenance & Evidence