Hydrochloric Acid → HCID 22485580, compound

Participants

Reaction Steps

To a solution of N,N-bis[N-[2-(3,4,5-trimethoxyphenyl)-5-pyridyl]-N-methyl-2-aminoethyl]methylamine (42.0 mg, 0.059 mmol) in ethanol (10 mL) was added 1.0 M hydrochloric acid (0.30 mL, 0.30 mmol), and the reaction mixture was concentrated under reduced pressure. Ethanol (10 mL) was added to the residue, and the mixture was concentrated under reduced pressure. The residue was recrystallized from ethanol-diethyl ether to yield the title compound as a yellow crystalline powder [melting point: 187.0° C. (decomposed)](37.1 mg, yield: 75%).

Provenance & Evidence