Hydrochloric Acid → HCID 22485612, compound

Participants

Reaction Steps

To a solution of N,N′-bis[2-(3,4,5-trimethoxyphenyl)-5-pyridyl]-N,N′-dimethyl-3-(1-pyrrolidinyl)-1,5-pentanediamine (49.6 mg, 0.0724 mmol) in ethanol (5.0 mL) was added 1.0 M hydrochloric acid solution (0.40 mL, 0.40 mmol), and the reaction mixture was concentrated under reduced pressure. Ethanol (10 mL) was added to the residue, and the resulting mixture was concentrated under reduced pressure to yield the title compound as a pale yellow amorphous powder (46.0 mg, yield: 71%).

Provenance & Evidence