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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2181368Generated: November 1, 2026

Toluene → HCID 21361290, compound

https://huagongshe.com/reaction/2181368

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTolueneHCID 1140—
ReactantTriethylamineHCID 8471—
ReactantHCID 22341826HCID 22341826—
ProductHCID 21361290HCID 2136129091%

Reaction Steps

In analogy to example 1 were reacted 6.1 g (2 mmol) of 2,2-diethyl-6,6-dimethyl-1-(1-phenyl-ethoxy)-piperidin-4-ol (prepared as described in GB 2335190, compound 110) with 4,38 g (2 mmol) of lauroyl chloride chloride and 2,02 g (2 mmol) of triethylamine in toluene to give 8,9 g (91%) dodecanoic acid 2,2-diethyl-6,6-dimethyl-1-(1-phenyl-ethoxy)-piperidin-4-yl ester as yellowish liquid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06891008B2
Source datasetuspto-grants-2005_05
ORD IDord-f923dd859c7b4b31a0537ecb70c922af
Source noteuspto-grants-2005_05