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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2181535Generated: November 1, 2026

HCID 21877361, compound → HCID 21877347, compound

https://huagongshe.com/reaction/2181535

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 21877361HCID 21877361—
ReactantHCID 21877448HCID 21877448—
ProductHCID 21877347HCID 2187734783%

Reaction Steps

[2-(4-Bromo-2-chloro-5-methyl-phenoxymethoxy)-ethyl]-trimethyl-silane was prepared in 83% yield from 4-bromo-3-chloro-5-methyl-phenol according to the procedure for [2-(4-bromo-2-methoxy-5-methyl-phenoxymethoxy)-ethyl]-trimethyl-silane. 1H NMR (300 MHz, CDCl3) δ 7.51 (s, 1H), 7.09 (s, 1H), 5.26 (s, 2H), 3.79 (t, 2H, J=8.4 Hz), 2.35 (s, 3H), 0.95 (t, 2H, J=8.4 Hz), 0.02 (s, 9H). Anal. (C13H20ClBrO2Si) C, H. Calculated: C, 44.39; H, 5.73. Found: C, 45.08; H, 5.91.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06891044B2
Source datasetuspto-grants-2005_05
ORD IDord-84d721632c504f2aad745a2a9b1fb939
Source noteuspto-grants-2005_05