HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → Benzene, ethenyl-, polymer with 1,3-butadiene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Chloric acid ethanol | HCID 21282719 | — |
| Product | Benzene, ethenyl-, polymer with 1,3-butadiene | HCID 62697 | — |
Reaction Steps
5 ml (50 μmol of Ti) of toluene solution in which the metallocene is dissolved was added while vigorously agitating. After agitating for 2 hours, 10 wt % of chloric acid-ethanol solution was added to terminate a reaction, the reactant was filtered, washed with ethanol and dried in a vacuum oven of 50° C. to obtain a final styrene/1,3-butadiene copolymer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06894129B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-9ce282f0268e4739bcc68be543347169 |
| Source note | uspto-grants-2005_05 |