Potassium Carbonate → 3-Chloro-5-[(2,4-dimethoxyphenyl)sulfonyl]-6-methyl-5,6-dihydrophenanthridine

Participants

Reaction Steps

The title compound was prepared from N-[1-(4′-chloro-2′-fluoro-1,1′-biphenyl-2-yl)ethyl]-2,4-dimethoxybenzenesulfonamide (470 mg, 1.04 mmol), anhydrous N,N-dimethylformamide (2 mL), and potassium carbonate (287 mg, 2.0 mmol) according to the procedure and in the same manner as described in Example 105, step d resulting in the isolation of 447 mg (100%) of a white solid that was used without further purification;

Provenance & Evidence