Perfluoropropionyl fluoride → HCID 11476181, compound

Participants

Reaction Conditions

Reaction Steps

HO(CH2)4OCH(CH3)CH2OH (18.8 g) obtained in Example 2-3 was put into a round bottom flask and stirred while maintaining the internal temperature at 30° C. Together with nitrogen, CF3CF2COF (276 g) was supplied over 6 hours while maintaining the internal temperature at 30° C. After completion of the reaction, stirring was continued for 2 hours at an internal temperature of 30° C. while supplying nitrogen gas, whereupon a 5% NaHCO3 aqueous solution (300 ml) was added at an internal temperature of at most 15° C.

Provenance & Evidence