Diethylene Glycol → HCID 89804272, compound

Participants

Reaction Conditions

Reaction Steps

HO(CH2)2O(CH2)2OH(40 g) was put into a flask and stirred while maintaining the internal temperature at 30° C. While maintaining the internal temperature of the flask at 30° C., nitrogen and CF3CF2COF (388 g) were supplied over a period of 1.5 hours. After completion of the reaction, while supplying nitrogen gas, stirring was continued at an internal temperature of 30° C. for 2 hours, and then the internal temperature of the flask was brought to at most 15° C., whereupon 5% NaHCO3 (300 ml) was added.

Provenance & Evidence