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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2182053Generated: November 1, 2026

3-Benzyloxybenzaldehyde → HCID 69381452, compound

https://huagongshe.com/reaction/2182053

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-BenzyloxybenzaldehydeHCID 74342—
Reactant1-Phenethylamine, (-)-HCID 75818—
Solventtert-Butyl methyl etherHCID 15413—
ProductHCID 69381452HCID 69381452115.5%

Reaction Steps

0.12 g (0.97 mmol) of (S)-α-methylbenzylamine and 0.25 g (1.19 mmol) of 3-benzyloxybenzaldehyde are mixed in 4 ml of t-butyl methyl ether and stirred for three days at room temperature, and then evaporated under reduced pressure to give 0.35 g (1.12 mmol) of (S)-N-(3-benzyloxybenzylidene)-α-methylbenzylamine (Yield: 115%, purity 85%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06894190B2
Source datasetuspto-grants-2005_05
ORD IDord-8f671be564a84a5d8c7a871d6fc13db3
Source noteuspto-grants-2005_05