HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Benzyloxybenzaldehyde → HCID 69381452, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Benzyloxybenzaldehyde | HCID 74342 | — |
| Reactant | 1-Phenethylamine, (-)- | HCID 75818 | — |
| Solvent | tert-Butyl methyl ether | HCID 15413 | — |
| Product | HCID 69381452 | HCID 69381452 | 115.5% |
Reaction Steps
0.12 g (0.97 mmol) of (S)-α-methylbenzylamine and 0.25 g (1.19 mmol) of 3-benzyloxybenzaldehyde are mixed in 4 ml of t-butyl methyl ether and stirred for three days at room temperature, and then evaporated under reduced pressure to give 0.35 g (1.12 mmol) of (S)-N-(3-benzyloxybenzylidene)-α-methylbenzylamine (Yield: 115%, purity 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06894190B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-8f671be564a84a5d8c7a871d6fc13db3 |
| Source note | uspto-grants-2005_05 |