HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-1-propanol → HCID 22478308, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-1-propanol | HCID 9086 | — |
| Reactant | 1,4-Dioxane-2,6-dione | HCID 78232 | — |
| Product | HCID 22478308 | HCID 22478308 | — |
Reaction Steps
A solution of diglycolic anhydride (2.32 g, 2/mmol) in 3-amino-1-propanol (6 ml) was refluxed a 180° C. for 3 hours. The volatiles were removed by evaporation a nd the residue was purified by column chromatography on silica eluting with methylene chloride/methanol (8/2) to give 4-(3-hydroxypropyl)-3,5-dioxomorpholine (3(46 g, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06897210B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-73af641e22b943f6a62c52511c9ee634 |
| Source note | uspto-grants-2005_05 |