HCID 22479199, compound → HCID 22479163, compound

Participants

Reaction Steps

The compound from Example 131 (100 mg) was dissolved in HBr (2 mL, 30% in AcOH). The resulting solution was stirred at room temperature for 30 minutes. The solution was extracted with EtOAc/H2O. The combined organic layers were dried over Na2SO4, filtered and evaporated. The product was purified by preparative TLC to yield the titled compound (52 mg). MS (m/z) 415 (MH+). mp. 103° C.

Provenance & Evidence