HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triethylamine → 2-Ethoxy-5-nitroquinoline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | o-Toluenesulfonyl chloride | HCID 8623 | — |
| Edukt | 5-Nitroquinoline 1-oxide | HCID 82085 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 2-Ethoxy-5-nitroquinoline | HCID 21948830 | — |
Reaktionsschritte
A suspension of 1 g (5 mmol) of 5-nitroquinoline-1-oxide, 1.23 g (6.4 mmol) of toluenesulfonic acid chloride and 1.4 ml (9.9 mmol) of triethylamine in 30 ml of EtOH is stirred for 60 hours at room temperature. The solid is suctioned off and washed with EtOH: 870 mg of product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06897224B2 |
| Quelldatensatz | uspto-grants-2005_05 |
| ORD ID | ord-050145125b3642e1aee1253746b3246d |
| Quellennotiz | uspto-grants-2005_05 |