HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22480224, compound → HCID 22480316, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22480224 | HCID 22480224 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22480316 | HCID 22480316 | 47% |
Reaction Steps
The title compound was prepared as described in Example 141 A, using 5-[(1 E)-2-pyridylvinyl]-3-(4-fluorophenyl)-1H-indazole (0.125 g, 0.4 mmol) in methanol and it was then purified by HPLC (0.060 g, 47% yield): 1H NMR (DMSO-d6) δ 13.14 (br s, 1H), 8.52 (d, 1H), 7.95 (m, 2H), 7.79 (s, 1H), 7.69 (ddd, 1H), 7.42 (dd, 1H), 7.22-7.35 (m, 5H), 3.12 (m, 4H); ES-MS (m/z) 318 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06897231B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-8953bb9024b74dfd99d8e7c4be89aed6 |
| Source note | uspto-grants-2005_05 |