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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2183219Generated: October 31, 2026

Triethylamine → HCID 22479700, compound

https://huagongshe.com/reaction/2183219

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantMethoxyacetyl chlorideHCID 96623—
ReactantHCID 22480146HCID 22480146—
SolventTetrahydrofuranHCID 8028—
ProductHCID 22479700HCID 22479700—

Reaction Steps

The title compound was prepared using 3-(3-aminophenyl)-1-perhydro-2H-pyran-2-yl-1H-indazole-5-carbonitrile (0.150 g, 0.47 mmol) in tetrahydrofuran (5 mL), 2-methoxy acetyl chloride (0.086 mL, 0.94 mmol) and triethyl amine (0.327 mL, 2.35 mmol). The crude product was isolated after partition of the reaction mixture between ethyl acetate and water. The yield was not calculated: ES-MS (m/z) 391 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06897231B2
Source datasetuspto-grants-2005_05
ORD IDord-9f7aad5182994c2586da2021e639497d
Source noteuspto-grants-2005_05