HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Thioglycolate → 4-Fluoro-1-benzothiophene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Thioglycolate | HCID 16907 | — |
| Reactant | 2,6-Difluorobenzaldehyde | HCID 136284 | — |
| Reactant | 4-Bromobenzo[b]thiophene | HCID 12094208 | — |
| Product | 4-Fluoro-1-benzothiophene | HCID 19088017 | — |
Reaction Steps
4-Fluorobenzo[b]thiophene was prepared starting from methyl thioglycolate and 2,6-difluorobenzaldehyde and then following a similar procedure to that given for 4-bromobenzo[b]thiophene in Example 9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06900216B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-1ce4e9a0b06f4b0e9b39d9e75ed03719 |
| Source note | uspto-grants-2005_05 |