HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 22472978, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 22472997 | HCID 22472997 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22472978 | HCID 22472978 | 131.7% |
Reaction Steps
To a solution of 5-(5-Nitro-pyridin-2-yloxy)-1-methyl-1H-indazole (0.79 mmol) in 10 mL of methanol was added 10 mL of ethyl acetate and 30 mg of platinum (IV) oxide. After shaking under 50 psi of H2 for 3 h, the mixture was filtered through a pad of Celite and concentrated in vacuo, affording 0.25 g of 5-(5-Amino-pyridin-2-yloxy)-1-methyl-1H-indazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06900201B2 |
| Source dataset | uspto-grants-2005_05 |
| ORD ID | ord-dc5e2e56fac044e3a5b527c91694048d |
| Source note | uspto-grants-2005_05 |